Selection of the HPLC Method in Chemical Analysis
Moldoveanu, Serban C.
David, Victor
Selection of the HPLC Method in Chemical Analysis serves as a practical guide to users of high performance liquid chromatography and provides exacting criteria for method selection, development, and validation. High performance liquid chromatography is the most common analytical technique currently practiced in chemistry. However, the process of finding the appropriate information for a particular analytical project requires significant effort and pre-existent knowledge in the field. Further, sorting through the wealth of published data and literature takes both time and effort away from the critical aspects of HPLC method selection. For the first time, a systematic approach for sorting through the available information and reviewing critically the up-to-date progress in HPLC for selecting a specific analysis is available in a single book. Selection of the HPLC Method in Chemical Analysis is an inclusive go-to reference for HPLC method selection, development, and validation. Addresses various aspects of practice and instrumentation needed to obtain reliable HPLC analysis resultsLeads researchers to the best choice of an HPLC method from the overabundance of information existent in the fieldProvides exacting criteria for HPLC method selection, development, and validation Authored by world-renowned HPLC experts who have more than 60 years of experience in the field combined INDICE: Chapter 1. Start of the implementation of a new HPLC method Chapter 2. Short overviews of analytical techniques not containing an independent separation step Chapter 3. Short overviews of main analytical techniques containing a separation step Chapter 4. Basic information regarding the HPLC techniques Chapter 5. Properties of analytes and matrices determining HPLC selection Chapter 6. General aspects regarding the HPLC analytical column Chapter 7. RP-HPLC analytical columns Chapter 8. Polar analytical columns Chapter 9. Stationary phases and columns for ion exchange, ion-moderated, and ligand exchange chromatography Chapter 10. Stationary phases and columns for chiral chromatography Chapter 11. Stationary phases and columns for size exclusion Chapter 12. Stationary phases and columns for immunoaffinity type separations Chapter 13. Solvents, buffers, and additives used in the mobile phase Chapter 14. Gradient elution Chapter 15. The Practice of HPLC Appendix 1. USP classification of HPLC columns Appendix 2. Hydrophobic stationary phases Appendix 3. HILIC and NPC stationary phases Appendix 4. Ion exchange and ion moderated stationary phases Appendix 5. Chiral stationary phases Appendix 6. Size exclusion stationary phases Appendix 7. Properties of mobile phase components
- ISBN: 978-0-12-803684-6
- Editorial: Elsevier
- Encuadernacion: Rústica
- Páginas: 550
- Fecha Publicación: 25/11/2016
- Nº Volúmenes: 1
- Idioma: Inglés